Mobile Phase
A: 2.72g NaOAc in 1000ml Water + 1.8ml TEA(pH=7.3) + 3ml THF
B: 2.72g NaOAc in 200ml Water + 400ml MeOH + 400ml ACN

Gradient(Flow):
0.00min flow - 0.45ml/min %B - 2%
1.00min  %B - 2%
17.00min %B - 60%
18.00min %B - 100%
18.10min flow - 0.8ml/min
23.90min flow - 0.8ml/min
24.00min flow - 0.45ml/min %B - 100%
25.00min flow - 0.45ml/min %B - 2%
30.00min Equilibrate

Temp: Room temperature
Detection: OPA / FMOC derivatisation